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How is vanadium oxychloride removed from titanium tetrachloride?
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titanium processing
High-purity (99.999 percent) titanium metal.
In the context of titanium processing, vanadium oxychloride is removed from titanium tetrachloride (TiCl₄) by reacting it with mineral oil. Because vanadium oxychloride has a boiling point similar to that of TiCl₄, it cannot be easily separated through standard distillation alone. The reaction with mineral oil effectively strips the impurity from the product stream, after which the TiCl₄ is redistilled in a reflux distillation column to achieve a purity exceeding 99.9 percent.1